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A quantitative method was developed for the direct infusion of samples for the analysis of di-, tri- and malto-saccharides (length of 4–10 monomers) that could be accomplished in one minute. A rapid and a simple method for the analysis of sugar which is applicable across diverse types of food matrices could be useful to the food industry in tackling the large number of the analysis required in various applications including nutritional labeling and also in reducing the extensive time currently required to complete this analysis.